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1. 西北工业大学超高温结构复合材料重点实验室
2. 山东工业陶瓷设计研究院
Published:2010
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白龙腾,成来飞,殷小玮,李向明,张立同,高芳. ZrO2 晶须增强多孔 ZrO2 陶瓷基复合材料的制备和性能[J]. 航空制造技术, 2010, 53(11): 76-79/84.
Preparation and Properties of Porous ZrOCeramic Matrix Composites Reinforced With ZrOWhisker[J]. Aeronautical Manufacturing Technology, 2010, 53(11): 76-79.
白龙腾,成来飞,殷小玮,李向明,张立同,高芳. ZrO2 晶须增强多孔 ZrO2 陶瓷基复合材料的制备和性能[J]. 航空制造技术, 2010, 53(11): 76-79/84. DOI: 10.16080/j.issn1671-833x.2010.11.021.
Preparation and Properties of Porous ZrOCeramic Matrix Composites Reinforced With ZrOWhisker[J]. Aeronautical Manufacturing Technology, 2010, 53(11): 76-79. DOI: 10.16080/j.issn1671-833x.2010.11.021.
以 ZrO(NO
3
)
2
·2H
O 和四方 ZrO
晶须为原料,采用醇 - 水溶液加热法并结合冷冻干燥法制备了多孔 ZrO
2(w)
/ZrO
陶瓷基复合材料。研究了四方 ZrO
晶须对多孔 ZrO
复合材料相成分、微结构、热导率及抗压强度的影响。结果表明, ZrO
晶须可以有效抑制 ZrO
由四方相转变为单斜相,当烧结温度为1 100℃时,多孔 ZrO
复合材料全部为四方相,其热导率远小于全部为单斜相的多孔 ZrO
陶瓷,抗压强度明显大于多孔 ZrO
陶瓷。
A ZrO(NO
O ceramic matrix composite is fabricated by using heating alcohol-aqueous solution and freeze-drying met hod with ZrO(NO
O and tetragonal ZrO
whisker as start materials. The effects of tetragonal ZrO
whisker on the phase composition
microstructure
thermal conductivity and compressive strength of porous ZrO
composite are investigated. The results indicate that ZrO
whisker could restrain the transformation of ZrO
from tetragonal to monoclinic effectively. When the sintering temperature
is 1 100℃
porous ZrO
composite is composed of tetragonal phase
and ZrO
ceramic is composed of monoclinic phase. The thermal conductivity of porous ZrO
composite is far less than that of porous ZrO
ceramic. And the compressive strength of porous ZrO
composite is much higher than that of porous ZrO
ceramic.
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