WANG Dongsheng, ZHANG Xiaodong, LIU Saiyue, WEI Fushuang, WANG You. Preparation and Characterization of Nano-Structured Mullite Feedstock[J]. Aeronautical Manufacturing Technology, 2023, 66(10): 72-76,84.
WANG Dongsheng, ZHANG Xiaodong, LIU Saiyue, WEI Fushuang, WANG You. Preparation and Characterization of Nano-Structured Mullite Feedstock[J]. Aeronautical Manufacturing Technology, 2023, 66(10): 72-76,84. DOI: 10.16080/j.issn1671-833x.2023.10.072.
Preparation and Characterization of Nano-Structured Mullite Feedstock
粉体为原材料,采用湿法球磨、喷雾干燥、固相烧结的方法制备了用于环境障涂层的纳米结构莫来石粉体喂料。借助X 射线衍射仪和扫描电镜研究了粉体喂料在不同热处理温度下的组织与形貌。结果显示,1300 ℃+150 min 的固相烧结的球形度与喷雾干燥所得的球形度保持一致,表面也较为光滑,缺陷较少,莫来石粉体喂料的粒径在60 μm 左右,晶粒为纳米结构。
Abstract
Environmental barrier coating (EBC) is a surface protection layer established between the service environment and the engine material to prevent or reduce the environmental erosion of the engine. Mullite is regarded as an important material for environmental barrier coating due to its good high temperature resistance
chemical compatibility, oxidation resistance and thermal conductivity. The preparation process of nanostructured mullite feedstock was studied
and the purpose was to prepare nanostructured feedstock with good sphericity
smooth surface
good fluidity and high density. This paper uses nano Al
2
O
3
and nano SiO
2
as raw materials
and uses spray drying and solid phase sinterin
g methods to prepare nanostructured mullite feedstock. The microstructure and morphology of feedstock at different heat treatment temperatures were studied by means of X-ray diffractometer and scanning electron microscopy. The experimental results show that the sphericity of solid-phase sintering at 1300 ℃ + 150 min is consistent with the sphericity of the feedstock obtained by spray drying