1. 大连理工大学高性能精密制造全国重点实验室,大连,116024
2. 沈阳芯源微电子设备股份有限公司,沈阳,110169
3. 中国人民解放军95939 部队,沧州,061736
纸质出版:2023
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吴东江,于学鑫,吕伟杰,石晶,由竹琳,马广义,牛方勇. 扫描速度对激光定向能量沉积Al2O3–ZrO2梯度陶瓷微观组织及力学性能的影响[J]. 航空制造技术, 2023, 66(16): 30-37.
WU Dongjiang, YU Xuexin, Lü Weijie, SHI Jing, YOU Zhulin, MA Guangyi, NIU Fangyong. Effect of Scanning Speed on Microstructure and Mechanical Properties of Al2O3–ZrO2 Gradient Ceramics Fabricated by Laser Directed Energy Deposition[J]. Aeronautical Manufacturing Technology, 2023, 66(16): 30-37.
吴东江,于学鑫,吕伟杰,石晶,由竹琳,马广义,牛方勇. 扫描速度对激光定向能量沉积Al2O3–ZrO2梯度陶瓷微观组织及力学性能的影响[J]. 航空制造技术, 2023, 66(16): 30-37. DOI: 0.16080/j.issn1671-833x.2023.16.030.
WU Dongjiang, YU Xuexin, Lü Weijie, SHI Jing, YOU Zhulin, MA Guangyi, NIU Fangyong. Effect of Scanning Speed on Microstructure and Mechanical Properties of Al2O3–ZrO2 Gradient Ceramics Fabricated by Laser Directed Energy Deposition[J]. Aeronautical Manufacturing Technology, 2023, 66(16): 30-37. DOI: 0.16080/j.issn1671-833x.2023.16.030.
功能梯度陶瓷作为能够兼顾结构和功能的新型陶瓷材料,其材料组成和性能可以根据需要呈现连续的梯度变化,因此在航空航天、生物医疗等领域具有广阔的应用前景。激光定向能量沉积技术克服了传统陶瓷制备方法在烧结变形及过渡界面明显的局限性,能够实现功能梯度陶瓷材料性能的区域可控制造。然而采用定工艺参数成形时,功能梯度陶瓷不同组分的性能无法同时达到最佳,因此就扫描速度对Al
2
O
3
–ZrO
2
梯度陶瓷中各比例复合陶瓷材料的影响规律展开了研究。在确定各比例复合陶瓷优选扫描速度的基础上,实现了Al
2
O
3
–ZrO
2
梯度陶瓷的变参数优化成形。结果表明,低速扫描条件下(200 mm/min、300 mm/min),α-Al
2
O
3
柱状晶定向生长倾向明显,但高ZrO
2
含量(质量分数)复合陶瓷材料宏观裂纹明显。扫描速度逐渐提高有助于晶粒尺寸减小,但过高的扫描速度(400 mm/min、500 mm/min)导致样件内部ZrO
2
团聚现象及孔隙缺陷增多。采用变扫描速度成形工艺不仅有效抑制了高ZrO
2
含量区域的宏观裂纹,而且改善了定参数成形Al
2
O
3
–ZrO
2
梯度陶瓷结合界面处的裂纹缺陷,优化成形的Al
2
O
3
–ZrO
2
梯度陶瓷结合界面处抗弯强度提升约21.37%。
Functional gradient ceramics (FGC) are novel ceramic materials that integrate structure and function
enabling the material’s composition and properties to continuously vary as needed. FGCs have broad application prospects in fields such as aerospace and biomedical engineering. Lase
r directed energy deposition (LDED) technique overcomes the obvious limitations of conventional preparation methods in terms of sintering deformation and transition interfaces
which achieves regionally controllable properties of FGCs. However
optimizing the performance of different components simultaneously through constant parameter fabrication is not feasible. Therefore
the effect of scanning speed on the composite ceramic materials with various proportions in Al
2
O
3
–ZrO
2
gradient ceramics was investigated. By determining the optimal scanning speed for each composite ceramic
the optimal fabrication of Al
2
O
3
–ZrO
2
gradient ceramics with variable parameters was achieved. The results show that under low scanning speed conditions (200 mm/min
300 mm/min)
the α-Al
2
O
3
columnar crystals exhibit obvious growth orientation tendency
and macroscopic cracks are apparent in composite ceramics with high ZrO
2
content. The gradual increase of scanning speed helps to reduce the grain size and thus improve the mechanical properties of the fabricated sample
but too high scanning speed leads to more internal defects and decreases the performance. The variable scanning speed fabricating process effectively suppresses the macroscopic cracks with high ZrO
2
content in the gradient region. In addition
the macro and micro cracking defects at the bonding interface of Al
2
O
3
–ZrO
2
gradient ceramics with constant parameters are improved. The flexural strength at the transition interface of optimally manufactured Al
2
O
3
–ZrO
2
gradient ceramics is improved by 21.37%.
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