WANG Cunshan,YU Qun. Mircrostructure and Properties of Nano-TiN-Ni45A Composite Coatings Prepared by Laser Cladding. Aeronautical Manufacturing Technology, 2016, 59(19): 39-44.
Ni-based composite coatings with different nano-TiN additions are produced by laser cladding on 38CrMoAl substrate. The influence of nano-TiN on the mircrostructure and properties of the coating is investigated through X-ray diffraction
scanning electron microscopy
electronic probe
Vickers hardness tester
and friction wear testing machine. Results show that the coatings consist of γ-Ni
Ni3B
M23C6
and TiN phases
exhibiting hypoeutectic morphological characteristics. As the addition of nano-TiN is 5.0 %
the primary γ-Ni dendrite is coarsed obviously
whose number is increased. However
as the addition of nano-TiN is more than 5.0 %
the primary γ-Ni dendrite shows decrases in size and number with increasing the addition of nano-TiN
whose growth morphology changes from equiaxed dendrite to columnar dendrite. Meanwhile
the number of the micron-sized TiN particle
growing in form of agglomeration
is also increased
and its distribution becomes more uniform. For this reason
the average hardness of the coatings gradually increases with increasing the addition of nano-TiN as a whole
and the tribological perperty is best as the addition of nano-TiN is 15%
showing 8.7% and 32.3% decrease in friction coefficient and wear volume as compared with the coating without TiN addition