1. 哈尔滨工业大学金属精密热加工国家级重点实验室,哈尔滨,150001
2. 哈尔滨工业大学空间环境材料行为与评价技术国家级重点实验室,哈尔滨,150001
纸质出版:2016
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丁宏升,李金韬,王 强,耿洪滨,陈瑞润,郭景杰,傅恒志. 冷坩埚定向凝固TiAl基合金高温持久性能研究*[J]. 航空制造技术, 2016, 59(23/24): 36-41. DING Hongsheng1, LI Jintao1, WANG Qiang1, GENG Hongbin2, CHEN Ruirun1,GUO Jingjie1, FU Hengzhi1. High Temperature Stress-Rupture Properties of TiAl Base Alloy Directionally Solidified by Cold Crucible Method. Aeronautical Manufacturing Technology, 2016, 59(23/24): 36-41.
DING Hongsheng, LI Jintao, WANG Qiang, et al. High Temperature Stress-Rupture Properties of TiAl Base Alloy Directionally Solidified by Cold Crucible Method[J]. Aeronautical Manufacturing Technology, 2016, 59(23/24).
丁宏升,李金韬,王 强,耿洪滨,陈瑞润,郭景杰,傅恒志. 冷坩埚定向凝固TiAl基合金高温持久性能研究*[J]. 航空制造技术, 2016, 59(23/24): 36-41. DING Hongsheng1, LI Jintao1, WANG Qiang1, GENG Hongbin2, CHEN Ruirun1,GUO Jingjie1, FU Hengzhi1. High Temperature Stress-Rupture Properties of TiAl Base Alloy Directionally Solidified by Cold Crucible Method. Aeronautical Manufacturing Technology, 2016, 59(23/24): 36-41. DOI: 10.16080/j.issn1671-833x.2016.23/24.036.
DING Hongsheng, LI Jintao, WANG Qiang, et al. High Temperature Stress-Rupture Properties of TiAl Base Alloy Directionally Solidified by Cold Crucible Method[J]. Aeronautical Manufacturing Technology, 2016, 59(23/24). DOI: 10.16080/j.issn1671-833x.2016.23/24.036.
采用电磁冷坩埚定向凝固技术制备了成分为Ti-47Al-2Cr-2Nb 的合金铸锭,定向凝固后的显微组织为α2+γ 全片层结构。在0.4~1.2mm/min 的抽拉速率范围内,随着抽拉速率的增加,片层间距减小,柱状晶与生长方向的夹角增大。随着温度升高,合金的拉伸强度有所下降,但由于细化片层界面对切变应力变形的阻碍作用,合金的高温拉伸强度会随着抽拉速率的增加而提高。通过对抽拉速率为1.0mm/min 试样的拉伸强度与温度的拟合,得到了拉伸强度和温度之间的函数关系。随着抽拉速率的增加,Ti-47Al-2Cr-2Nb 合金的持久寿命明显升高,对于抽拉速率为1.2mm/min 试样的持久性能测试表明,其持久寿命最长,达到了48h。持久试样的断口形貌表明,其断裂的主要方式是伴随着少量延性断裂的脆性解理断裂。最后根据时间- 温度模型,分别采用Larson-Miller 和Manson-Haferd 参数法建立了定向凝固Ti-47Al-2Cr-2Nb 合金的持久强度预测函数模型,预测的理论值与试验结果吻合度较高。
In this paper
TiAl based alloy with composition of Ti-47Al-2Cr-2Nb has been successfully prepared by electromagnetic cold crucible directional solidification. The microstructure of the directionally solidified alloy consisted of alternatively arranged lamellae which were composed of α2+γ laths. The inter-lamellar spacing was influenced by withdrawal rate and thinner inter-lamellar spacing was achieved at higher withdrawal rate. The included angels between columnar crystal orientation and the growth direction increase with the increasing withdrawal rate. The high temperature tensile properties were tested from 600℃ to 800℃ and the fracture strength of the alloy decreased with the increasing test temperature. Inter-lamellar spacing was a significant influence factor on the high temperature tensile strength and the alloy prepared at withdrawal rate of 1.2mm/min showed the highest strength (470MPa) at 800℃ . The α2/γ interfaces in the fully lamellar structure could act as obstacles to shearing. Higher density of interfaces existed in the matrix of the alloy with higher withdrawal rates and greater applied stress was essential for further deformation in case of thinner inter-lamellar spacing. A function of tensile strength and test temperature was created according to the values of alloy prepared at withdrawal rate of 1.0 mm/min from 600℃ to 800℃ . The effect of withdrawal rate on the stress rupture-properties was investigated at 200MPa/650℃ . The results showed that finer inter-lamellar spacing could enhance the high temperature stress ruptureproperties. Under the same test conditions
the alloy prepared at withdrawal rate of 1.2mm/min held the highest creeprupture life (48h). The improvement effect of thinner lamellar structure on creep-rupture life decreased with the increasing test temperature and applied stress. The fracture morphology of the stress-rupture samples indicated the Ti-47Al-2Cr-2Nb behaved in brittle cleavage fracture companied with a small amount of ductile fracture. The predication model of the stressrupture was set up through Larson-Miller and Manson-Haferd parametric method. The predication function is an accurate model confirmed by little difference existing between theoretical and experimental values.
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