CHEN Shiqi, LIU Lianping. Effects of Particle Size on Microstructures and Properties of GH4169 Alloy by SLM Additive Manufacturing. 航空制造技术, 2021, 64(9): 14-20.
CHEN Shiqi, LIU Lianping. Effects of Particle Size on Microstructures and Properties of GH4169 Alloy by SLM Additive Manufacturing. 航空制造技术, 2021, 64(9): 14-20. DOI: 10.16080/j.issn1671-833x.2021.09.014.
为探究 GH4169 合金原始粉末粒度对增材制造(Additive manufacturing, AM)成形件组织与性能的影响,选取两种不同粒度范围的合金粉末进行选区激光熔化(Selective laser melting,SLM)试验,并进行相同条件的热处理。测试了沉积态和热处理态的密度和室温拉伸性能,观察了金相组织、断口形貌以及热处理后的析出相。结果表明:粗粉沉积态密度大于细粉沉积态,粉末粒度显著影响制件力学性能,细粉可以适当提高热处理态屈服强度 R
p0.2
和抗拉强度 R
m
,粗粉得到更高的断后伸长率 A。沉积态试样沿沉积方向呈现鱼鳞状熔池,细粉沉积态中不规则熔池多于粗粉;熔池凝固从熔池界面开始,继承已凝固熔池的组织特征,呈现组织遗传现象,粉末粒度对沉积态组织结构无明显影响;热处理态组织均为等轴晶,降低沉积态组织缺陷,析出强化相,是 R
p0.2
和 R
m
提高的原因。
Abstract
To investigate the influence of raw GH4169 alloy particle size on microstructures and properties of AM moldings
two kinds of alloy powder with different particle size range were selected for selective laser melting experiment
and samples were heat treated under the same conditions. Density and tensile properties were analyzed for both as-deposited and heat-treated samples. All samples’ microstructures
fracture morphologies and precipitates were observed by OM and SEM. The results indicate that the density of coarse powder in as-deposited samples is higher than that of fine powder
and samples with fine powder have higher yiel
d strength R
p0.2
and tensile strength R
m
in heat-treated. However
as-deposited and heat-treated samples with coarse powder exhibit higher elongation. What’s more
the as-deposited samples’ molten pool has a configuration of fish scales along the deposition direction
and samples with fine powder have more irregular molten pools than coarse powder. Meanwhile
solidification of molten pool starts from interface and inherits the structural characteristics of solidified molten pool
possessing structure genetic characteristic. Microstructure of both samples shows no significant difference
indicating the size of powder particles has no obvious effects on their microstructures. The equiaxed grain microstructures formed after the heat treatment reduce defects