1. 中国航空制造技术研究院,北京,100024
2. 高能束流加工技术重点实验室,北京,100024
纸质出版:2019
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张雪峰,李怀学,胡全栋,巩水利. 热处理对激光选区熔化GH4169高温合金的组织与拉伸性能的影响[J]. 航空制造技术, 2019, 62(19): 78-85.
ZHANG Xuefeng, LI Huaixue, HU Quandong, GONG Shuili. Effect of Heat Treatment on the Microstructure and Tensile Properties of GH4169 Superalloy Fabricated by Selective Laser Melting. Aeronautical Manufacturing Technology, 2019, 62(19): 78-85.
张雪峰,李怀学,胡全栋,巩水利. 热处理对激光选区熔化GH4169高温合金的组织与拉伸性能的影响[J]. 航空制造技术, 2019, 62(19): 78-85. DOI: 10.16080/j.issn1671–833x.2019.19.078.
ZHANG Xuefeng, LI Huaixue, HU Quandong, GONG Shuili. Effect of Heat Treatment on the Microstructure and Tensile Properties of GH4169 Superalloy Fabricated by Selective Laser Melting. Aeronautical Manufacturing Technology, 2019, 62(19): 78-85. DOI: 10.16080/j.issn1671–833x.2019.19.078.
采用激光选区熔化技术成形了GH4169 高温合金试样。研究了固溶加双时效热处理(1060℃/1h 炉冷+760℃/8h 炉冷2h 至650℃/8h,炉冷) 对沉积态GH4169 高温合金的显微组织与拉伸性能的影响,并对沉积态组织特征和热处理析出相进行了表征。结果表明:在基板平面方向,GH4169 沉积态组织表现为细小的“ 胞状” 晶粒结构, 而在平行于沉积方向截面,沉积态组织形貌为呈一定外延生长的柱状枝晶结构。由于成形过程中极快的冷却速度,沉积态下强化相的析出被抑制,其组织主要表征为过饱和的奥氏体基体γ 和枝晶间γ+Laves 共晶。经过固溶加双时效热处理,沉积态中胞状枝晶与Laves 相溶解,在晶界处析出片状δ 相,在晶粒内部析出弥散分布的圆盘状γ″ 相和圆粒状γ′ 相。热处理工艺改善了沉积态试样的拉伸强度,在析出相强化的作用下,GH4169 热处理态试样的室温拉伸性能达到锻件水平。
The GH4169 superalloy samples were fabricated by selective laser melting. The effects of solution plus double aging heat treatment on the microstructures and tensile properties of selective laser melted GH4169 samples have been investigated. The microstructure of as-deposited GH4169 samples and precipitations after heat treatment were characterized. In the horizontal section (normal to the deposition direction)
the as-deposited sample occurs a fine cellular grains structure
while in the vertical section (parallel to the deposition direction)
the as-deposited microstructure shows a dendritic structure with a certain epitaxial growth feature. The precipitation of the strengthening phase is inhibited due to the fast cooling rate
thus the microstructure of as-deposited GH4169 sample is characterized by supersaturated austenite matrix γ and inter-dendritic γ + Laves eutectic. After solution plus double aging heat treatment
the dendritic grains and Laves phase dissolved in the austenite matrix. The plate-like δ phase precipitates at the grain boundary
and the discshaped γ"-Ni3Nb phase and the granular γ'-Ni3 (Al
Ti) phase are dispersed inside the grains. The tensile strength of the asdeposited sample are improved after heat treatment. Under the effect of precipitation strengthening
the tensile properties of the heat-treated GH4169 sample at room temperature are comparable to those of forgings.
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